Analytical Chemistry – Laboratory / CHEM 3232

Instructor: Dr. Mihaela Leonida

Text: R.A. Day and A.L. Underwood, Quantitative Analysis, 6th ed.
 
Week
 Experiment Title 
Exp. #
1
Check-in

Errors. Stoichiometry. Calculations.

 
2
Standardization of NaOH solutions w/ KHPhtalate 
Titration of antiacids 
3.3 & 3.8
3
 Standardization of HCl solution with Na2CO3
Determination of the alkalinity of soda ash 
3.4 & 3.7
4
Preparation and standardization of Na-EDTA solution 
Determination of the total hardness of water
5.6 & 5.7
5
Preparation and standardization of 0.1 N I2
solution with As2O3
Determination of vitamin C
4.12 & 4.14
6
Determination of glucose
7.5
7
HPLC
10.4
8
Electrolytic determination of copper
9.1
9
Separation of Cu and Ni by electrolysis
9.2
10
Identification of an amino acid
8.4
11
 Determination of dopamine in beers. "Bananatrode"
hand-out
12
Spectroscopy of crepe paper dyes
Spectroanalysis of a paint sample
hand-out
13
Analysis of nitrite in water
Check-out
7.3

 

Grading Policy

Experimental work                            50 %
Results (accuracy, precision)             20 %
Lab report                                        30 %